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Electrochemical analysis is critical skill to teach in chemistry curricula since it is a crucial tool in current high-impact chemistry research. Electrochemistry enables researchers to analysis a variety of systems prolonging from molecule to products that include research themes varying from clean energy to substrate activation in organic systems. Specifically, it can reveal information about catalytic efficiency, the function of catalysts, and also the nature of chemical reduction and oxidation (redox) processes. Researchers working in the area that catalysis rely heavily on electrochemistry, utilizing it to identify reliable catalysts and also optimize reaction conditions. This laboratory experiment starts with an introduce tutorial come electrochemistry by guiding students through the usage of numerous electrochemical techniques using the ferricyanide/ferrocyanide redox couple as a version system. The methods covered in the tutorial incorporate cyclic voltammetry, differential pulse voltammetry, Tafel analysis, and bulk electrolysis. The protocol then uses these techniques to electrocatalysis through identifying and also characterizing catalysts because that hydrogen and also oxygen generation in the water electrolysis reaction. Electrochemical methods are connected to present chemical research study by concentrating on catalysis in the context of renewable energy, i m sorry is a present societal and curricular imperative. The entire laboratory protocol described herein is carried out in teams of 2 to 3 students in a four hour laboratory duration and is an ideal for upper-level physical, analytical, or not natural chemistry.